Single layer glass reactor is also called vacuum reactor or multifunctional reactor, which can complete a variety of solvent synthesis reactions under high temperature conditions. The single-layer glass reactor usually has its own heating function, which is generally divided into two types: high-temperature bath pot and heating sleeve. Users can choose according to their own needs.
Assembly steps of single-layer glass reactor:
1. Carefully check whether the accessories are complete and damaged according to the packing list.
2. The stainless steel bracket shall be assembled according to the instructions.
3. The vertical pole of the support is used to fix the support and electrical part of the kettle body, and the single-layer reactor generally has two vertical poles.
4. The kettle body bracket is fixed on the upright according to the use height, and the kettle body is placed on the bracket. Pay attention to ensure that the reactor body is vertical.
5. The mixing rod is installed on the gear ring collet of the motor spindle. The mixing rod passes through the rotating bearing of the shaft cap, fastens the special joint, and then adjusts the position of the motor. Note that the center of the circle is vertical to the kettle body.
6. Install the electric box and vacuum meter on the top of the other pole, and tighten the screws.
7. The left standard port on the kettle cover is used to insert the serpentine reflux condenser, the right side is the feeding port to connect the constant pressure funnel, and the middle front standard port is the casing to insert the thermometer.
8. When installing the glassware, it must be clean. Each interface of the glassware can be coated with Vaseline to prevent the glass from being stuck. Finally, vacuum grease can be coated to increase the air tightness.
9. Fix the universal wheel and insert the power supply for mixing. If the mixing is stable and smooth, it means that the installation and commissioning have been completed.
